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#=AR# <br />ANALYTICAL RESULTS <br />Pace Project No.: <br />Project: <br />10650001 <br />B2204011.00-Revised Report <br />Sample: Pond 3-E Lab ID: 10650001005 Collected: 04/18/23 12:45 Received: 04/18/23 16:07 Matrix: Solid <br />Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. <br />Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL <br />Analytical Method: EPA 6020B Preparation Method: EPA 3050B <br />Pace Analytical Services - Minneapolis <br />6020B MET ICPMS <br />Arsenic 1.3 mg/kg 04/24/23 18:30 7440-38-204/23/23 06:340.73 0.21 1 <br />Copper 9.4 mg/kg 04/24/23 18:30 7440-50-804/23/23 06:341.5 0.44 1 <br />Analytical Method: ASTM D2974 <br />Pace Analytical Services - Minneapolis <br />Dry Weight / %M by ASTM D2974 <br />Percent Moisture 31.5 % 04/20/23 12:26 N20.10 0.10 1 <br />Analytical Method: EPA 8270E by SIM Preparation Method: EPA 3546 <br />Pace Analytical Services - Minneapolis <br />8270E MSSV CPAH by SIM <br />Acenaphthene <1.9 ug/kg 04/27/23 18:54 83-32-904/21/23 13:2013.9 1.9 1 <br />Acenaphthylene <1.6 ug/kg 04/27/23 18:54 208-96-804/21/23 13:2013.9 1.6 1 <br />Anthracene 24.0 ug/kg 04/27/23 18:54 120-12-704/21/23 13:2013.9 1.5 1 <br />Benzo(a)anthracene 137 ug/kg 04/27/23 18:54 56-55-304/21/23 13:2013.9 3.8 1 <br />Benzo(a)pyrene 146 ug/kg 04/27/23 18:54 50-32-804/21/23 13:2013.9 1.8 1 <br />Benzo(g,h,i)perylene 108 ug/kg 04/27/23 18:54 191-24-204/21/23 13:2013.9 2.9 1 <br />Benzofluoranthenes (Total)282 ug/kg 04/27/23 18:54 N204/21/23 13:2041.7 8.6 1 <br />Chrysene 169 ug/kg 04/27/23 18:54 218-01-904/21/23 13:2013.9 2.5 1 <br />Dibenz(a,h)acridine <1.6 ug/kg 04/27/23 18:54 226-36-804/21/23 13:2013.9 1.6 1 <br />Dibenz(a,h)anthracene 23.1 ug/kg 04/27/23 18:54 53-70-304/21/23 13:2013.9 1.1 1 <br />Dibenzo(a,e)pyrene 50.8 ug/kg 04/27/23 18:54 192-65-404/21/23 13:2013.9 1.6 1 <br />Dibenzo(a,h)pyrene 27.5 ug/kg 04/27/23 18:54 189-64-004/21/23 13:2013.9 2.8 1 <br />Dibenzo(a,i)pyrene 15.9 ug/kg 04/27/23 18:54 189-55-904/21/23 13:2013.9 1.3 1 <br />Dibenzo(a,l)pyrene <2.0 ug/kg 04/27/23 18:54 191-30-0 L204/21/23 13:2013.9 2.0 1 <br />7H-Dibenzo(c,g)carbazole <5.7 ug/kg 04/27/23 18:54 194-59-204/21/23 13:2013.9 5.7 1 <br />7,12-Dimethylbenz(a)anthracene <0.67 ug/kg 04/27/23 18:54 57-97-604/21/23 13:2013.9 0.67 1 <br />Fluoranthene 376 ug/kg 04/27/23 18:54 206-44-004/21/23 13:2013.9 3.4 1 <br />Fluorene <1.9 ug/kg 04/27/23 18:54 86-73-704/21/23 13:2013.9 1.9 1 <br />Indeno(1,2,3-cd)pyrene 116 ug/kg 04/27/23 18:54 193-39-504/21/23 13:2013.9 1.3 1 <br />3-Methylcholanthrene <3.2 ug/kg 04/27/23 18:54 56-49-5 L204/21/23 13:2013.9 3.2 1 <br />5-Methylchrysene 18.7 ug/kg 04/27/23 18:54 3697-24-304/21/23 13:2013.9 1.8 1 <br />2-Methylnaphthalene <2.5 ug/kg 04/27/23 18:54 91-57-604/21/23 13:2013.9 2.5 1 <br />Naphthalene <2.7 ug/kg 04/27/23 18:54 91-20-304/21/23 13:2013.9 2.7 1 <br />Phenanthrene 172 ug/kg 04/27/23 18:54 85-01-804/21/23 13:2013.9 2.4 1 <br />Pyrene 287 ug/kg 04/27/23 18:54 129-00-004/21/23 13:2013.9 3.2 1 <br />Surrogates <br />2-Fluorobiphenyl (S) 85 %. 04/27/23 18:54 321-60-804/21/23 13:2046-125 1 <br />p-Terphenyl-d14 (S) 89 %. 04/27/23 18:54 1718-51-004/21/23 13:2069-125 1 <br />REPORT OF LABORATORY ANALYSIS <br />This report shall not be reproduced, except in full, <br />without the written consent of Pace Analytical Services, LLC.Date: 05/02/2023 11:28 AM <br />Pace Analytical Services, LLC <br />1700 Elm Street <br />Minneapolis, MN 55414 <br />(612)607-1700 <br />Page 12 of 24