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06-23-25-SWS
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#=QC# <br />QUALITY CONTROL DATA <br />Pace Project No.: <br />Project: <br />10732220 <br />B2502087 2026 PMP Inprovements <br />Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. <br />QC Batch: <br />QC Batch Method: <br />Analysis Method: <br />Analysis Description: <br />1003652 <br />EPA 3546 <br />EPA 8270E by SIM <br />8270E Solid PAH by SIM MSSV <br />Laboratory:Pace Analytical Services - Minneapolis <br />Associated Lab Samples:10732220001, 10732220002, 10732220003, 10732220004, 10732220005 <br />Parameter Units <br />Blank <br />Result <br />Reporting <br />Limit Qualifiers <br />METHOD BLANK:5234083 <br />Associated Lab Samples:10732220001, 10732220002, 10732220003, 10732220004, 10732220005 <br />Matrix:Solid <br />AnalyzedMDL <br />2-Methylnaphthalene ug/kg <3.7 10.0 04/29/25 02:273.7 <br />Acenaphthene ug/kg <1.0 10.0 04/29/25 02:271.0 <br />Acenaphthylene ug/kg <1.0 10.0 04/29/25 02:271.0 <br />Anthracene ug/kg <1.8 10.0 04/29/25 02:271.8 <br />Benzo(g,h,i)perylene ug/kg <3.8 10.0 04/29/25 02:273.8 <br />Fluoranthene ug/kg <2.7 10.0 04/29/25 02:272.7 <br />Fluorene ug/kg <1.4 10.0 04/29/25 02:271.4 <br />Naphthalene ug/kg <2.7 10.0 04/29/25 02:272.7 <br />Phenanthrene ug/kg <2.5 10.0 04/29/25 02:272.5 <br />Pyrene ug/kg <3.0 10.0 04/29/25 02:273.0 <br />2-Fluorobiphenyl (S)%.72 39-125 04/29/25 02:27 <br />p-Terphenyl-d14 (S)%.91 41-125 04/29/25 02:27 <br />Parameter Units <br />LCS <br />Result <br />% Rec <br />Limits Qualifiers% RecConc. <br />5234084LABORATORY CONTROL SAMPLE: <br />LCSSpike <br />2-Methylnaphthalene ug/kg 70.6100 71 45-125 <br />Acenaphthene ug/kg 68.6100 69 54-125 <br />Acenaphthylene ug/kg 69.8100 70 53-125 <br />Anthracene ug/kg 73.7100 74 61-125 <br />Benzo(g,h,i)perylene ug/kg 90.3100 90 60-125 <br />Fluoranthene ug/kg 72.0100 72 64-125 <br />Fluorene ug/kg 69.2100 69 56-125 <br />Naphthalene ug/kg 64.6100 65 51-125 <br />Phenanthrene ug/kg 67.2100 67 61-125 <br />Pyrene ug/kg 86.5100 86 62-125 <br />2-Fluorobiphenyl (S)%.71 39-125 <br />p-Terphenyl-d14 (S)%.91 41-125 <br />Parameter Units <br />MS <br />Result <br />% Rec <br />Limits Qual% RecConc. <br />5234085MATRIX SPIKE & MATRIX SPIKE DUPLICATE: <br />MSSpike <br />Result <br />10732220001 <br />5234086 <br />MSD <br />Result <br />MSD <br />% Rec RPD RPD <br />Max <br />MSDMS <br />Spike <br />Conc. <br />2-Methylnaphthalene ug/kg 122 72 30-15063 13 30122<22.8 87.7 77.2 <br />Acenaphthene ug/kg 122 63 31-12562 1 3012220.1J 96.5 95.5 <br />Acenaphthylene ug/kg 122 69 38-12562 9 3012213.1J 97.4 88.8 <br />Anthracene ug/kg 122 35 30-15044 9 3012268.4 111 122 <br />REPORT OF LABORATORY ANALYSIS <br />This report shall not be reproduced, except in full, <br />without the written consent of Pace Analytical Services, LLC.Date: 05/05/2025 06:54 AM <br />Pace Analytical Services, LLC <br />1700 Elm Street <br />Minneapolis, MN 55414 <br />(612)607-1700 <br />Page 15 of 23
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