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<br />'-1 <br />,. <br />;J <br /> <br />~J <br /> <br />Emission Test Report <br />EMC W A-2-08 <br />Section 4 <br />Revision: 0 <br />Date: September 30, 1999 <br />Page lof9 <br /> <br />I <br />I <br />r-'-.~. <br />h... <br />i <br />t..... <br /> <br />Section 4. <br />Sampling, Analytical, and Process Data Collection <br />Procedures <br /> <br />"l <br />1:1 <br />~ ..! <br /> <br />The sampling, analysis, and process data collection procedures used for this test <br />project are described in this section. The published methods and MRI Standard Operating <br />Procedures (SOPs) used are cited. Details providing clarification and any modifications to <br />or deviations from the published methods are presented in this section. Otherwise, the <br />cited methods were followed. <br /> <br />Cl <br />o <br /> <br />4.1 Sampling Procedures <br /> <br />The samples collected required the uSe of four (4) sampling systems at both sampling <br />locations: <br /> <br />~--\ <br /> <br />I .I <br /> <br />· EPA Method 23 isokinetic sampling train for PCDDs and PCDFs, along with an <br />EPA Method 3B integrated gas sampling train for carbon dioxide (C02) and <br />oxygen (OJ. <br /> <br />u <br />] <br />f") <br />~] <br /> <br />· EP A Method 29 isokinetic sampling train for metals (Cd, Hg, and Pb), along with <br />an EP A Method 3B integrated gas sampling train. <br /> <br />· EP A Method 26A isokinetic sampling train for PM and HCl, along with an EP A <br />Method 3B integrated gas sampling train. <br /> <br />c-, <br /> <br />LJ <br /> <br />· EPA Instrumental Analyzer Methods 6C, 7E, and 10 sampling and analytical <br />system for S02, NOx, and CO. Method 3A instrumentation was also added for <br />CO2 and O2 data collection for nonnalizing the S02' NOx, and CO results if <br />needed. <br /> <br />The following methods were employed in the use and operation of these sampling <br />trains and systems. <br /> <br />11 <br />, I <br />I,.J <br /> <br />4.1.1 Sample and Velocity Traverses <br /> <br />n <br />u <br /> <br />Method 1 in Appendix A of 40 CFR 60 (basis for MRI SOP MRI-8401) was used to <br />establish traverse (sampling) points at the test locations for the traversing sampling trains. <br /> <br />i I <br /> <br />~_J <br /> <br />MRI-AED\R49S 1-08-03 54. wpd <br /> <br />ctC\ <br />q :'7D - <br />