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#=AR# <br />ANALYTICAL RESULTS <br />Pace Project No.: <br />Project: <br />10650001 <br />B2204011.00-Revised Report <br />Sample: Pond 1-E Lab ID: 10650001001 Collected: 04/18/23 09:50 Received: 04/18/23 16:07 Matrix: Solid <br />Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. <br />Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL <br />Analytical Method: EPA 6020B Preparation Method: EPA 3050B <br />Pace Analytical Services - Minneapolis <br />6020B MET ICPMS <br />Arsenic 3.1 mg/kg 04/24/23 18:13 7440-38-204/23/23 06:340.69 0.20 1 <br />Copper 9.4 mg/kg 04/24/23 18:13 7440-50-804/23/23 06:341.4 0.42 1 <br />Analytical Method: ASTM D2974 <br />Pace Analytical Services - Minneapolis <br />Dry Weight / %M by ASTM D2974 <br />Percent Moisture 28.9 % 04/20/23 11:41 N20.10 0.10 1 <br />Analytical Method: EPA 8270E by SIM Preparation Method: EPA 3546 <br />Pace Analytical Services - Minneapolis <br />8270E MSSV CPAH by SIM <br />Acenaphthene <1.9 ug/kg 04/27/23 15:54 83-32-904/21/23 13:2013.8 1.9 1 <br />Acenaphthylene 15.2 ug/kg 04/27/23 15:54 208-96-804/21/23 13:2013.8 1.6 1 <br />Anthracene 7.7J ug/kg 04/27/23 15:54 120-12-704/21/23 13:2013.8 1.5 1 <br />Benzo(a)anthracene 76.7 ug/kg 04/27/23 15:54 56-55-304/21/23 13:2013.8 3.8 1 <br />Benzo(a)pyrene 79.0 ug/kg 04/27/23 15:54 50-32-804/21/23 13:2013.8 1.8 1 <br />Benzo(g,h,i)perylene 98.2 ug/kg 04/27/23 15:54 191-24-204/21/23 13:2013.8 2.9 1 <br />Benzofluoranthenes (Total)239 ug/kg 04/27/23 15:54 N204/21/23 13:2041.5 8.5 1 <br />Chrysene 134 ug/kg 04/27/23 15:54 218-01-9 M104/21/23 13:2013.8 2.5 1 <br />Dibenz(a,h)acridine <1.6 ug/kg 04/27/23 15:54 226-36-804/21/23 13:2013.8 1.6 1 <br />Dibenz(a,h)anthracene 18.2 ug/kg 04/27/23 15:54 53-70-304/21/23 13:2013.8 1.1 1 <br />Dibenzo(a,e)pyrene 38.5 ug/kg 04/27/23 15:54 192-65-404/21/23 13:2013.8 1.6 1 <br />Dibenzo(a,h)pyrene 21.2 ug/kg 04/27/23 15:54 189-64-004/21/23 13:2013.8 2.8 1 <br />Dibenzo(a,i)pyrene <1.3 ug/kg 04/27/23 15:54 189-55-904/21/23 13:2013.8 1.3 1 <br />Dibenzo(a,l)pyrene <2.0 ug/kg 04/27/23 15:54 191-30-0 L204/21/23 13:2013.8 2.0 1 <br />7H-Dibenzo(c,g)carbazole <5.7 ug/kg 04/27/23 15:54 194-59-204/21/23 13:2013.8 5.7 1 <br />7,12-Dimethylbenz(a)anthracene <0.66 ug/kg 04/27/23 15:54 57-97-6 M104/21/23 13:2013.8 0.66 1 <br />Fluoranthene 222 ug/kg 04/27/23 15:54 206-44-0 M104/21/23 13:2013.8 3.3 1 <br />Fluorene <1.9 ug/kg 04/27/23 15:54 86-73-704/21/23 13:2013.8 1.9 1 <br />Indeno(1,2,3-cd)pyrene 96.2 ug/kg 04/27/23 15:54 193-39-504/21/23 13:2013.8 1.3 1 <br />3-Methylcholanthrene <3.2 ug/kg 04/27/23 15:54 56-49-5 L204/21/23 13:2013.8 3.2 1 <br />5-Methylchrysene 11.3J ug/kg 04/27/23 15:54 3697-24-304/21/23 13:2013.8 1.8 1 <br />2-Methylnaphthalene <2.5 ug/kg 04/27/23 15:54 91-57-604/21/23 13:2013.8 2.5 1 <br />Naphthalene <2.6 ug/kg 04/27/23 15:54 91-20-304/21/23 13:2013.8 2.6 1 <br />Phenanthrene 62.7 ug/kg 04/27/23 15:54 85-01-804/21/23 13:2013.8 2.4 1 <br />Pyrene 170 ug/kg 04/27/23 15:54 129-00-0 M104/21/23 13:2013.8 3.2 1 <br />Surrogates <br />2-Fluorobiphenyl (S) 77 %. 04/27/23 15:54 321-60-804/21/23 13:2046-125 1 <br />p-Terphenyl-d14 (S) 84 %. 04/27/23 15:54 1718-51-004/21/23 13:2069-125 1 <br />REPORT OF LABORATORY ANALYSIS <br />This report shall not be reproduced, except in full, <br />without the written consent of Pace Analytical Services, LLC.Date: 05/02/2023 11:28 AM <br />Pace Analytical Services, LLC <br />1700 Elm Street <br />Minneapolis, MN 55414 <br />(612)607-1700 <br />Page 8 of 24