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#=AR# ANALYTICAL RESULTS Pace Project No.: Project: 10650001 B2204011.00-Revised Report Sample: Pond 1-W Lab ID: 10650001002 Collected: 04/18/23 10:15 Received: 04/18/23 16:07 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL Analytical Method: EPA 6020B Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis 6020B MET ICPMS Arsenic 4.6 mg/kg 04/24/23 18:16 7440-38-204/23/23 06:340.87 0.25 1 Copper 20.3 mg/kg 04/24/23 18:16 7440-50-804/23/23 06:341.7 0.53 1 Analytical Method: ASTM D2974 Pace Analytical Services - Minneapolis Dry Weight / %M by ASTM D2974 Percent Moisture 45.1 % 04/20/23 11:41 N20.10 0.10 1 Analytical Method: EPA 8270E by SIM Preparation Method: EPA 3546 Pace Analytical Services - Minneapolis 8270E MSSV CPAH by SIM Acenaphthene <2.4 ug/kg 04/27/23 17:24 83-32-904/21/23 13:2018.0 2.4 1 Acenaphthylene <2.1 ug/kg 04/27/23 17:24 208-96-804/21/23 13:2018.0 2.1 1 Anthracene <1.9 ug/kg 04/27/23 17:24 120-12-704/21/23 13:2018.0 1.9 1 Benzo(a)anthracene 42.0 ug/kg 04/27/23 17:24 56-55-304/21/23 13:2018.0 4.9 1 Benzo(a)pyrene 49.2 ug/kg 04/27/23 17:24 50-32-804/21/23 13:2018.0 2.3 1 Benzo(g,h,i)perylene 39.9 ug/kg 04/27/23 17:24 191-24-204/21/23 13:2018.0 3.8 1 Benzofluoranthenes (Total)106 ug/kg 04/27/23 17:24 N204/21/23 13:2053.9 11.1 1 Chrysene 61.1 ug/kg 04/27/23 17:24 218-01-904/21/23 13:2018.0 3.3 1 Dibenz(a,h)acridine <2.0 ug/kg 04/27/23 17:24 226-36-804/21/23 13:2018.0 2.0 1 Dibenz(a,h)anthracene <1.4 ug/kg 04/27/23 17:24 53-70-304/21/23 13:2018.0 1.4 1 Dibenzo(a,e)pyrene 19.8 ug/kg 04/27/23 17:24 192-65-404/21/23 13:2018.0 2.0 1 Dibenzo(a,h)pyrene <3.6 ug/kg 04/27/23 17:24 189-64-004/21/23 13:2018.0 3.6 1 Dibenzo(a,i)pyrene <1.7 ug/kg 04/27/23 17:24 189-55-904/21/23 13:2018.0 1.7 1 Dibenzo(a,l)pyrene <2.6 ug/kg 04/27/23 17:24 191-30-0 L204/21/23 13:2018.0 2.6 1 7H-Dibenzo(c,g)carbazole <7.4 ug/kg 04/27/23 17:24 194-59-204/21/23 13:2018.0 7.4 1 7,12-Dimethylbenz(a)anthracene <0.86 ug/kg 04/27/23 17:24 57-97-604/21/23 13:2018.0 0.86 1 Fluoranthene 132 ug/kg 04/27/23 17:24 206-44-004/21/23 13:2018.0 4.3 1 Fluorene <2.4 ug/kg 04/27/23 17:24 86-73-704/21/23 13:2018.0 2.4 1 Indeno(1,2,3-cd)pyrene 42.1 ug/kg 04/27/23 17:24 193-39-504/21/23 13:2018.0 1.7 1 3-Methylcholanthrene <4.1 ug/kg 04/27/23 17:24 56-49-5 L204/21/23 13:2018.0 4.1 1 5-Methylchrysene <2.3 ug/kg 04/27/23 17:24 3697-24-304/21/23 13:2018.0 2.3 1 2-Methylnaphthalene <3.3 ug/kg 04/27/23 17:24 91-57-604/21/23 13:2018.0 3.3 1 Naphthalene <3.4 ug/kg 04/27/23 17:24 91-20-304/21/23 13:2018.0 3.4 1 Phenanthrene 38.7 ug/kg 04/27/23 17:24 85-01-804/21/23 13:2018.0 3.1 1 Pyrene 102 ug/kg 04/27/23 17:24 129-00-004/21/23 13:2018.0 4.1 1 Surrogates 2-Fluorobiphenyl (S) 83 %. 04/27/23 17:24 321-60-804/21/23 13:2046-125 1 p-Terphenyl-d14 (S) 86 %. 04/27/23 17:24 1718-51-004/21/23 13:2069-125 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/02/2023 11:28 AM Pace Analytical Services, LLC 1700 Elm Street Minneapolis, MN 55414 (612)607-1700 Page 9 of 24