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#=AR# ANALYTICAL RESULTS Pace Project No.: Project: 10650001 B2204011.00-Revised Report Sample: Pond 2-W Lab ID: 10650001003 Collected: 04/18/23 11:00 Received: 04/18/23 16:07 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL Analytical Method: EPA 6020B Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis 6020B MET ICPMS Arsenic 1.2 mg/kg 04/24/23 18:25 7440-38-204/23/23 06:340.69 0.20 1 Copper 13.5 mg/kg 04/24/23 18:25 7440-50-804/23/23 06:341.4 0.42 1 Analytical Method: ASTM D2974 Pace Analytical Services - Minneapolis Dry Weight / %M by ASTM D2974 Percent Moisture 29.4 % 04/20/23 11:41 N20.10 0.10 1 Analytical Method: EPA 8270E by SIM Preparation Method: EPA 3546 Pace Analytical Services - Minneapolis 8270E MSSV CPAH by SIM Acenaphthene <1.8 ug/kg 04/27/23 17:54 83-32-904/21/23 13:2013.6 1.8 1 Acenaphthylene <1.6 ug/kg 04/27/23 17:54 208-96-804/21/23 13:2013.6 1.6 1 Anthracene <1.5 ug/kg 04/27/23 17:54 120-12-704/21/23 13:2013.6 1.5 1 Benzo(a)anthracene <3.7 ug/kg 04/27/23 17:54 56-55-304/21/23 13:2013.6 3.7 1 Benzo(a)pyrene <1.7 ug/kg 04/27/23 17:54 50-32-804/21/23 13:2013.6 1.7 1 Benzo(g,h,i)perylene <2.9 ug/kg 04/27/23 17:54 191-24-204/21/23 13:2013.6 2.9 1 Benzofluoranthenes (Total)29.8J ug/kg 04/27/23 17:54 N204/21/23 13:2040.7 8.3 1 Chrysene 17.2 ug/kg 04/27/23 17:54 218-01-904/21/23 13:2013.6 2.5 1 Dibenz(a,h)acridine <1.5 ug/kg 04/27/23 17:54 226-36-804/21/23 13:2013.6 1.5 1 Dibenz(a,h)anthracene <1.1 ug/kg 04/27/23 17:54 53-70-304/21/23 13:2013.6 1.1 1 Dibenzo(a,e)pyrene <1.5 ug/kg 04/27/23 17:54 192-65-404/21/23 13:2013.6 1.5 1 Dibenzo(a,h)pyrene <2.7 ug/kg 04/27/23 17:54 189-64-004/21/23 13:2013.6 2.7 1 Dibenzo(a,i)pyrene <1.3 ug/kg 04/27/23 17:54 189-55-904/21/23 13:2013.6 1.3 1 Dibenzo(a,l)pyrene <1.9 ug/kg 04/27/23 17:54 191-30-0 L204/21/23 13:2013.6 1.9 1 7H-Dibenzo(c,g)carbazole <5.6 ug/kg 04/27/23 17:54 194-59-204/21/23 13:2013.6 5.6 1 7,12-Dimethylbenz(a)anthracene <0.65 ug/kg 04/27/23 17:54 57-97-604/21/23 13:2013.6 0.65 1 Fluoranthene 32.9 ug/kg 04/27/23 17:54 206-44-004/21/23 13:2013.6 3.3 1 Fluorene <1.8 ug/kg 04/27/23 17:54 86-73-704/21/23 13:2013.6 1.8 1 Indeno(1,2,3-cd)pyrene <1.3 ug/kg 04/27/23 17:54 193-39-504/21/23 13:2013.6 1.3 1 3-Methylcholanthrene <3.1 ug/kg 04/27/23 17:54 56-49-5 L204/21/23 13:2013.6 3.1 1 5-Methylchrysene <1.7 ug/kg 04/27/23 17:54 3697-24-304/21/23 13:2013.6 1.7 1 2-Methylnaphthalene <2.5 ug/kg 04/27/23 17:54 91-57-604/21/23 13:2013.6 2.5 1 Naphthalene <2.6 ug/kg 04/27/23 17:54 91-20-304/21/23 13:2013.6 2.6 1 Phenanthrene <2.3 ug/kg 04/27/23 17:54 85-01-804/21/23 13:2013.6 2.3 1 Pyrene 20.0 ug/kg 04/27/23 17:54 129-00-004/21/23 13:2013.6 3.1 1 Surrogates 2-Fluorobiphenyl (S) 78 %. 04/27/23 17:54 321-60-804/21/23 13:2046-125 1 p-Terphenyl-d14 (S) 73 %. 04/27/23 17:54 1718-51-004/21/23 13:2069-125 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/02/2023 11:28 AM Pace Analytical Services, LLC 1700 Elm Street Minneapolis, MN 55414 (612)607-1700 Page 10 of 24