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#=QC# <br />QUALITY CONTROL DATA <br />Pace Project No.: <br />Project: <br />10650001 <br />B2204011.00-Revised Report <br />Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. <br />QC Batch: <br />QC Batch Method: <br />Analysis Method: <br />Analysis Description: <br />876844 <br />EPA 3546 <br />EPA 8270E by SIM <br />8270E Solid PAH by SIM MSSV <br />Laboratory: Pace Analytical Services - Minneapolis <br />Associated Lab Samples: 10650001001, 10650001002, 10650001003, 10650001004, 10650001005, 10650001006 <br />Parameter Units <br />Blank <br />Result <br />Reporting <br />Limit Qualifiers <br />METHOD BLANK: 4623732 <br />Associated Lab Samples:10650001001, 10650001002, 10650001003, 10650001004, 10650001005, 10650001006 <br />Matrix: Solid <br />AnalyzedMDL <br />2-Methylnaphthalene ug/kg <1.8 10.0 04/27/23 15:241.8 <br />3-Methylcholanthrene ug/kg <2.3 10.0 04/27/23 15:242.3 <br />5-Methylchrysene ug/kg <1.3 10.0 04/27/23 15:241.3 <br />7,12-Dimethylbenz(a)anthracene ug/kg <0.48 10.0 04/27/23 15:240.48 <br />7H-Dibenzo(c,g)carbazole ug/kg <4.1 10.0 04/27/23 15:244.1 <br />Acenaphthene ug/kg <1.3 10.0 04/27/23 15:241.3 <br />Acenaphthylene ug/kg <1.2 10.0 04/27/23 15:241.2 <br />Anthracene ug/kg <1.1 10.0 04/27/23 15:241.1 <br />Benzo(a)anthracene ug/kg <2.7 10.0 04/27/23 15:242.7 <br />Benzo(a)pyrene ug/kg <1.3 10.0 04/27/23 15:241.3 <br />Benzo(g,h,i)perylene ug/kg <2.1 10.0 04/27/23 15:242.1 <br />Benzofluoranthenes (Total) ug/kg <6.2 30.0 N204/27/23 15:246.2 <br />Chrysene ug/kg <1.8 10.0 04/27/23 15:241.8 <br />Dibenz(a,h)acridine ug/kg <1.1 10.0 04/27/23 15:241.1 <br />Dibenz(a,h)anthracene ug/kg <0.79 10.0 04/27/23 15:240.79 <br />Dibenzo(a,e)pyrene ug/kg <1.1 10.0 04/27/23 15:241.1 <br />Dibenzo(a,h)pyrene ug/kg <2.0 10.0 04/27/23 15:242.0 <br />Dibenzo(a,i)pyrene ug/kg <0.97 10.0 04/27/23 15:240.97 <br />Dibenzo(a,l)pyrene ug/kg <1.4 10.0 04/27/23 15:241.4 <br />Fluoranthene ug/kg <2.4 10.0 04/27/23 15:242.4 <br />Fluorene ug/kg <1.3 10.0 04/27/23 15:241.3 <br />Indeno(1,2,3-cd)pyrene ug/kg <0.97 10.0 04/27/23 15:240.97 <br />Naphthalene ug/kg <1.9 10.0 04/27/23 15:241.9 <br />Phenanthrene ug/kg <1.7 10.0 04/27/23 15:241.7 <br />Pyrene ug/kg <2.3 10.0 04/27/23 15:242.3 <br />2-Fluorobiphenyl (S) %. 83 46-125 04/27/23 15:24 <br />p-Terphenyl-d14 (S) %. 95 69-125 04/27/23 15:24 <br />Parameter Units <br />LCS <br />Result <br />% Rec <br />Limits Qualifiers% RecConc. <br />4623733LABORATORY CONTROL SAMPLE: <br />LCSSpike <br />2-Methylnaphthalene ug/kg 251300 84 70-130 <br />3-Methylcholanthrene ug/kg 96.4 L2300 32 70-130 <br />5-Methylchrysene ug/kg 272300 91 70-130 <br />7,12-Dimethylbenz(a)anthracene ug/kg 216300 72 70-130 <br />7H-Dibenzo(c,g)carbazole ug/kg 279300 93 70-130 <br />Acenaphthene ug/kg 247300 82 70-130 <br />Acenaphthylene ug/kg 245300 82 70-130 <br />Anthracene ug/kg 253300 84 70-130 <br />REPORT OF LABORATORY ANALYSIS <br />This report shall not be reproduced, except in full, <br />without the written consent of Pace Analytical Services, LLC.Date: 05/02/2023 11:28 AM <br />Pace Analytical Services, LLC <br />1700 Elm Street <br />Minneapolis, MN 55414 <br />(612)607-1700 <br />Page 17 of 24