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#=QC# <br />QUALITY CONTROL DATA <br />Pace Project No.: <br />Project: <br />10650001 <br />B2204011.00-Revised Report <br />Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. <br />Parameter Units <br />LCS <br />Result <br />% Rec <br />Limits Qualifiers% RecConc. <br />4623733LABORATORY CONTROL SAMPLE: <br />LCSSpike <br />Benzo(a)anthracene ug/kg 259300 86 70-130 <br />Benzo(a)pyrene ug/kg 274300 91 70-130 <br />Benzo(g,h,i)perylene ug/kg 289300 96 70-130 <br />Benzofluoranthenes (Total) ug/kg 884 N2900 98 70-130 <br />Chrysene ug/kg 264300 88 70-130 <br />Dibenz(a,h)acridine ug/kg 302300 101 70-130 <br />Dibenz(a,h)anthracene ug/kg 299300 100 70-130 <br />Dibenzo(a,e)pyrene ug/kg 270300 90 70-130 <br />Dibenzo(a,h)pyrene ug/kg 294300 98 70-130 <br />Dibenzo(a,i)pyrene ug/kg 245300 82 70-130 <br />Dibenzo(a,l)pyrene ug/kg 92.2 L2300 31 70-130 <br />Fluoranthene ug/kg 266300 89 70-130 <br />Fluorene ug/kg 260300 87 70-130 <br />Indeno(1,2,3-cd)pyrene ug/kg 294300 98 70-130 <br />Naphthalene ug/kg 246300 82 70-130 <br />Phenanthrene ug/kg 266300 89 70-130 <br />Pyrene ug/kg 263300 88 70-130 <br />2-Fluorobiphenyl (S) %. 84 46-125 <br />p-Terphenyl-d14 (S) %. 95 69-125 <br />Parameter Units <br />MS <br />Result <br />% Rec <br />Limits Qual% RecConc. <br />4623734MATRIX SPIKE & MATRIX SPIKE DUPLICATE: <br />MSSpike <br />Result <br />10650001001 <br />4623735 <br />MSD <br />Result <br />MSD <br />% Rec RPD RPD <br />Max <br />MSDMS <br />Spike <br />Conc. <br />2-Methylnaphthalene ug/kg 404 81 70-13081 5 30421<2.5 325 342 <br />3-Methylcholanthrene ug/kg 404 76 70-13085 15 30421<3.2 309 358 <br />5-Methylchrysene ug/kg 404 86 70-13086 4 3042111.3J 358 374 <br />7,12- <br />Dimethylbenz(a)anthracene <br />ug/kg M1404 37 70-13029 21 30421<0.66 148 120 <br />7H-Dibenzo(c,g)carbazole ug/kg 404 102 70-130101 3 30421<5.7 413 425 <br />Acenaphthene ug/kg 404 85 70-13084 3 30421<1.9 343 352 <br />Acenaphthylene ug/kg 404 80 70-13079 2 3042115.2 338 347 <br />Anthracene ug/kg 404 84 70-13083 3 304217.7J 346 358 <br />Benzo(a)anthracene ug/kg 404 72 70-13076 7 3042176.7 367 396 <br />Benzo(a)pyrene ug/kg 404 79 70-13083 7 3042179.0 399 428 <br />Benzo(g,h,i)perylene ug/kg 404 75 70-13076 5 3042198.2 399 418 <br />Benzofluoranthenes (Total) ug/kg N21210 76 70-13077 4 301260239 1160 1210 <br />Chrysene ug/kg M1404 58 70-13063 8 30421134 369 400 <br />Dibenz(a,h)acridine ug/kg 404 98 70-13096 2 30421<1.6 395 403 <br />Dibenz(a,h)anthracene ug/kg 404 93 70-13092 4 3042118.2 392 406 <br />Dibenzo(a,e)pyrene ug/kg 404 79 70-13079 3 3042138.5 359 372 <br />Dibenzo(a,h)pyrene ug/kg 404 94 70-13095 5 3042121.2 402 421 <br />Dibenzo(a,i)pyrene ug/kg 404 92 70-13094 5 30421<1.3 373 394 <br />Dibenzo(a,l)pyrene ug/kg 404 72 70-13081 15 30421<2.0 291 339 <br />Fluoranthene ug/kg M1404 47 70-13058 12 30421222 412 465 <br />REPORT OF LABORATORY ANALYSIS <br />This report shall not be reproduced, except in full, <br />without the written consent of Pace Analytical Services, LLC.Date: 05/02/2023 11:28 AM <br />Pace Analytical Services, LLC <br />1700 Elm Street <br />Minneapolis, MN 55414 <br />(612)607-1700 <br />Page 18 of 24