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#=AR# <br />ANALYTICAL RESULTS <br />Pace Project No.: <br />Project: <br />10732220 <br />B2502087 2026 PMP Inprovements <br />Sample:O-1 Lab ID:10732220001 Collected:04/24/25 11:45 Received:04/24/25 16:40 Matrix:Solid <br />Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. <br />Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL <br />Analytical Method: ASTM D2974 <br />Pace Analytical Services - Minneapolis <br />Dry Weight / %M by ASTM D2974 <br />Percent Moisture 19.2 %04/28/25 09:24 N20.10 0.10 1 <br />Analytical Method: EPA 8270E by SIM Preparation Method: EPA 3546 <br />Pace Analytical Services - Minneapolis <br />8270E MSSV PAH by SIM <br />Acenaphthene 20.1J ug/kg 04/29/25 08:53 83-32-904/28/25 14:4461.2 6.4 5 <br />Acenaphthylene 13.1J ug/kg 04/29/25 08:53 208-96-804/28/25 14:4461.2 6.1 5 <br />Anthracene 68.4 ug/kg 04/29/25 08:53 120-12-704/28/25 14:4461.2 10.8 5 <br />Benzo(g,h,i)perylene 237 ug/kg 04/29/25 08:53 191-24-2 M104/28/25 14:4461.2 23.5 5 <br />Fluoranthene 872 ug/kg 04/29/25 08:53 206-44-0 M1,R104/28/25 14:4461.2 16.3 5 <br />Fluorene 37.5J ug/kg 04/29/25 08:53 86-73-704/28/25 14:4461.2 8.6 5 <br />2-Methylnaphthalene <22.8 ug/kg 04/29/25 08:53 91-57-604/28/25 14:4461.2 22.8 5 <br />Naphthalene <16.3 ug/kg 04/29/25 08:53 91-20-304/28/25 14:4461.2 16.3 5 <br />Phenanthrene 453 ug/kg 04/29/25 08:53 85-01-8 M104/28/25 14:4461.2 15.3 5 <br />Pyrene 734 ug/kg 04/29/25 08:53 129-00-0 M1,R104/28/25 14:4461.2 18.2 5 <br />Surrogates <br />2-Fluorobiphenyl (S)69 %.04/29/25 08:53 321-60-8 ED04/28/25 14:4439-125 5 <br />p-Terphenyl-d14 (S)79 %.04/29/25 08:53 1718-51-004/28/25 14:4441-125 5 <br />Analytical Method: EPA 8270E by SIM Preparation Method: EPA 3546 <br />Pace Analytical Services - Minneapolis <br />8270E MSSV CPAH by SIM <br />Benzo(a)anthracene 86.3 ug/kg 04/30/25 02:44 56-55-3 R104/29/25 13:5224.5 8.9 2 <br />Benzo(a)pyrene 100 ug/kg 04/30/25 02:44 50-32-8 R104/29/25 13:5224.5 9.3 2 <br />Benzofluoranthenes (Total)211 ug/kg 04/30/25 02:44 N204/29/25 13:5273.6 23.8 2 <br />Chrysene 124 ug/kg 04/30/25 02:44 218-01-9 R104/29/25 13:5224.5 7.2 2 <br />Dibenz(a,h)acridine <8.4 ug/kg 04/30/25 02:44 226-36-804/29/25 13:5224.5 8.4 2 <br />Dibenz(a,h)anthracene 15.5J ug/kg 04/30/25 02:44 53-70-304/29/25 13:5224.5 8.5 2 <br />Dibenzo(a,e)pyrene 18.4J ug/kg 04/30/25 02:44 192-65-404/29/25 13:5224.5 6.9 2 <br />Dibenzo(a,h)pyrene 9.4J ug/kg 04/30/25 02:44 189-64-0 M104/29/25 13:5224.5 6.8 2 <br />Dibenzo(a,i)pyrene <8.2 ug/kg 04/30/25 02:44 189-55-9 M104/29/25 13:5224.5 8.2 2 <br />Dibenzo(a,l)pyrene <5.4 ug/kg 04/30/25 02:44 191-30-0 M104/29/25 13:5224.5 5.4 2 <br />7H-Dibenzo(c,g)carbazole <7.7 ug/kg 04/30/25 02:44 194-59-204/29/25 13:5224.5 7.7 2 <br />7,12-Dimethylbenz(a)anthracene <7.1 ug/kg 04/30/25 02:44 57-97-604/29/25 13:5224.5 7.1 2 <br />Indeno(1,2,3-cd)pyrene 75.4 ug/kg 04/30/25 02:44 193-39-5 R104/29/25 13:5224.5 8.2 2 <br />3-Methylcholanthrene <5.3 ug/kg 04/30/25 02:44 56-49-504/29/25 13:5224.5 5.3 2 <br />5-Methylchrysene <6.6 ug/kg 04/30/25 02:44 3697-24-304/29/25 13:5224.5 6.6 2 <br />Surrogates <br />2-Fluorobiphenyl (S)70 %.04/30/25 02:44 321-60-8 ED04/29/25 13:5245-125 2 <br />p-Terphenyl-d14 (S)78 %.04/30/25 02:44 1718-51-004/29/25 13:5253-125 2 <br />REPORT OF LABORATORY ANALYSIS <br />This report shall not be reproduced, except in full, <br />without the written consent of Pace Analytical Services, LLC.Date: 05/05/2025 06:54 AM <br />Pace Analytical Services, LLC <br />1700 Elm Street <br />Minneapolis, MN 55414 <br />(612)607-1700 <br />Page 9 of 23