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#=AR# <br />ANALYTICAL RESULTS <br />Pace Project No.: <br />Project: <br />10732220 <br />B2502087 2026 PMP Inprovements <br />Sample:O-2 Lab ID:10732220002 Collected:04/24/25 11:00 Received:04/24/25 16:40 Matrix:Solid <br />Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. <br />Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL <br />Analytical Method: ASTM D2974 <br />Pace Analytical Services - Minneapolis <br />Dry Weight / %M by ASTM D2974 <br />Percent Moisture 25.0 %04/28/25 09:26 N20.10 0.10 1 <br />Analytical Method: EPA 8270E by SIM Preparation Method: EPA 3546 <br />Pace Analytical Services - Minneapolis <br />8270E MSSV PAH by SIM <br />Acenaphthene 935 ug/kg 04/29/25 10:01 83-32-904/28/25 14:4464.5 6.8 5 <br />Acenaphthylene 392 ug/kg 04/29/25 10:01 208-96-804/28/25 14:4464.5 6.4 5 <br />Anthracene 3580 ug/kg 04/29/25 10:01 120-12-704/28/25 14:4464.5 11.4 5 <br />Benzo(g,h,i)perylene 7500 ug/kg 04/29/25 17:59 191-24-204/28/25 14:4464524850 <br />Fluoranthene 33000 ug/kg 04/29/25 17:59 206-44-004/28/25 14:4464517250 <br />Fluorene 2110 ug/kg 04/29/25 10:01 86-73-704/28/25 14:4464.5 9.1 5 <br />2-Methylnaphthalene 80.9 ug/kg 04/29/25 10:01 91-57-604/28/25 14:4464.5 24.1 5 <br />Naphthalene 234 ug/kg 04/29/25 10:01 91-20-304/28/25 14:4464.5 17.2 5 <br />Phenanthrene 19800 ug/kg 04/29/25 17:59 85-01-804/28/25 14:4464516150 <br />Pyrene 26500 ug/kg 04/29/25 17:59 129-00-004/28/25 14:4464519250 <br />Surrogates <br />2-Fluorobiphenyl (S)69 %.04/29/25 10:01 321-60-8 D404/28/25 14:4439-125 5 <br />p-Terphenyl-d14 (S)83 %.04/29/25 10:01 1718-51-004/28/25 14:4441-125 5 <br />Analytical Method: EPA 8270E by SIM Preparation Method: EPA 3546 <br />Pace Analytical Services - Minneapolis <br />8270E MSSV CPAH by SIM <br />Benzo(a)anthracene 5360 ug/kg 05/02/25 15:59 56-55-304/29/25 13:5232911925 <br />Benzo(a)pyrene 5770 ug/kg 05/02/25 15:59 50-32-804/29/25 13:5232912525 <br />Benzofluoranthenes (Total)18700 ug/kg 04/30/25 04:46 N204/29/25 13:5219863.9 5 <br />Chrysene 7140 ug/kg 05/02/25 15:59 218-01-904/29/25 13:5232996.5 25 <br />Dibenz(a,h)acridine 260 ug/kg 04/30/25 04:46 226-36-804/29/25 13:5265.9 22.5 5 <br />Dibenz(a,h)anthracene 817 ug/kg 04/30/25 04:46 53-70-304/29/25 13:5265.9 22.9 5 <br />Dibenzo(a,e)pyrene 703 ug/kg 04/30/25 04:46 192-65-404/29/25 13:5265.9 18.6 5 <br />Dibenzo(a,h)pyrene 316 ug/kg 04/30/25 04:46 189-64-004/29/25 13:5265.9 18.1 5 <br />Dibenzo(a,i)pyrene 80.0 ug/kg 04/30/25 04:46 189-55-904/29/25 13:5265.9 22.0 5 <br />Dibenzo(a,l)pyrene 50.2J ug/kg 04/30/25 04:46 191-30-004/29/25 13:5265.9 14.4 5 <br />7H-Dibenzo(c,g)carbazole 93.2 ug/kg 04/30/25 04:46 194-59-204/29/25 13:5265.9 20.6 5 <br />7,12-Dimethylbenz(a)anthracene <19.0 ug/kg 04/30/25 04:46 57-97-604/29/25 13:5265.9 19.0 5 <br />Indeno(1,2,3-cd)pyrene 3810 ug/kg 04/30/25 04:46 193-39-504/29/25 13:5265.9 22.0 5 <br />3-Methylcholanthrene 102 ug/kg 04/30/25 04:46 56-49-504/29/25 13:5265.9 14.1 5 <br />5-Methylchrysene <17.8 ug/kg 04/30/25 04:46 3697-24-304/29/25 13:5265.9 17.8 5 <br />Surrogates <br />2-Fluorobiphenyl (S)68 %.04/30/25 04:46 321-60-8 ED04/29/25 13:5245-125 5 <br />p-Terphenyl-d14 (S)79 %.04/30/25 04:46 1718-51-004/29/25 13:5253-125 5 <br />REPORT OF LABORATORY ANALYSIS <br />This report shall not be reproduced, except in full, <br />without the written consent of Pace Analytical Services, LLC.Date: 05/05/2025 06:54 AM <br />Pace Analytical Services, LLC <br />1700 Elm Street <br />Minneapolis, MN 55414 <br />(612)607-1700 <br />Page 10 of 23