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#=AR# <br />ANALYTICAL RESULTS <br />Pace Project No.: <br />Project: <br />10732220 <br />B2502087 2026 PMP Inprovements <br />Sample:O-3 Lab ID:10732220003 Collected:04/24/25 10:30 Received:04/24/25 16:40 Matrix:Solid <br />Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. <br />Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL <br />Analytical Method: ASTM D2974 <br />Pace Analytical Services - Minneapolis <br />Dry Weight / %M by ASTM D2974 <br />Percent Moisture 31.1 %04/28/25 09:30 N20.10 0.10 1 <br />Analytical Method: EPA 8270E by SIM Preparation Method: EPA 3546 <br />Pace Analytical Services - Minneapolis <br />8270E MSSV PAH by SIM <br />Acenaphthene 1050 ug/kg 04/29/25 10:24 83-32-904/28/25 14:4471.6 7.5 5 <br />Acenaphthylene 150 ug/kg 04/29/25 10:24 208-96-804/28/25 14:4471.6 7.2 5 <br />Anthracene 3570 ug/kg 04/29/25 10:24 120-12-704/28/25 14:4471.6 12.7 5 <br />Benzo(g,h,i)perylene 10700 ug/kg 04/29/25 18:21 191-24-204/28/25 14:4471627550 <br />Fluoranthene 43000 ug/kg 04/29/25 18:21 206-44-004/28/25 14:4471619050 <br />Fluorene 1730 ug/kg 04/29/25 10:24 86-73-704/28/25 14:4471.6 10.1 5 <br />2-Methylnaphthalene 37.8J ug/kg 04/29/25 10:24 91-57-604/28/25 14:4471.6 26.7 5 <br />Naphthalene 66.4J ug/kg 04/29/25 10:24 91-20-304/28/25 14:4471.6 19.0 5 <br />Phenanthrene 22200 ug/kg 04/29/25 18:21 85-01-804/28/25 14:4471617950 <br />Pyrene 35500 ug/kg 04/29/25 18:21 129-00-004/28/25 14:4471621350 <br />Surrogates <br />2-Fluorobiphenyl (S)65 %.04/29/25 10:24 321-60-8 D404/28/25 14:4439-125 5 <br />p-Terphenyl-d14 (S)83 %.04/29/25 10:24 1718-51-004/28/25 14:4441-125 5 <br />Analytical Method: EPA 8270E by SIM Preparation Method: EPA 3546 <br />Pace Analytical Services - Minneapolis <br />8270E MSSV CPAH by SIM <br />Benzo(a)anthracene 11600 ug/kg 05/02/25 16:30 56-55-304/29/25 13:5235712925 <br />Benzo(a)pyrene 12900 ug/kg 05/02/25 16:30 50-32-804/29/25 13:5235713525 <br />Benzofluoranthenes (Total)25600 ug/kg 05/02/25 16:30 N204/29/25 13:52107034725 <br />Chrysene 16000 ug/kg 05/02/25 16:30 218-01-904/29/25 13:5235710525 <br />Dibenz(a,h)acridine 551 ug/kg 04/30/25 05:17 226-36-804/29/25 13:5271.5 24.4 5 <br />Dibenz(a,h)anthracene 1820 ug/kg 04/30/25 05:17 53-70-304/29/25 13:5271.5 24.8 5 <br />Dibenzo(a,e)pyrene 1530 ug/kg 04/30/25 05:17 192-65-404/29/25 13:5271.5 20.2 5 <br />Dibenzo(a,h)pyrene 690 ug/kg 04/30/25 05:17 189-64-004/29/25 13:5271.5 19.7 5 <br />Dibenzo(a,i)pyrene 183 ug/kg 04/30/25 05:17 189-55-904/29/25 13:5271.5 23.9 5 <br />Dibenzo(a,l)pyrene 95.1 ug/kg 04/30/25 05:17 191-30-004/29/25 13:5271.5 15.6 5 <br />7H-Dibenzo(c,g)carbazole 208 ug/kg 04/30/25 05:17 194-59-204/29/25 13:5271.5 22.3 5 <br />7,12-Dimethylbenz(a)anthracene <20.7 ug/kg 04/30/25 05:17 57-97-604/29/25 13:5271.5 20.7 5 <br />Indeno(1,2,3-cd)pyrene 9620 ug/kg 05/02/25 16:30 193-39-504/29/25 13:5235711925 <br />3-Methylcholanthrene 311 ug/kg 04/30/25 05:17 56-49-504/29/25 13:5271.5 15.3 5 <br />5-Methylchrysene <19.3 ug/kg 04/30/25 05:17 3697-24-304/29/25 13:5271.5 19.3 5 <br />Surrogates <br />2-Fluorobiphenyl (S)68 %.04/30/25 05:17 321-60-8 ED04/29/25 13:5245-125 5 <br />p-Terphenyl-d14 (S)82 %.04/30/25 05:17 1718-51-004/29/25 13:5253-125 5 <br />REPORT OF LABORATORY ANALYSIS <br />This report shall not be reproduced, except in full, <br />without the written consent of Pace Analytical Services, LLC.Date: 05/05/2025 06:54 AM <br />Pace Analytical Services, LLC <br />1700 Elm Street <br />Minneapolis, MN 55414 <br />(612)607-1700 <br />Page 11 of 23