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Emission Test Report p <br /> EMC WA-2-08 <br /> Section 5 <br /> Revision: 0 <br /> Date: September 30, 1999 <br /> Page 4 of 18 <br /> Table 5-2. Criteria for Ein"ssion Measurement and Data Quality <br /> Test MOW of <br /> rerneters Matrix determination Fn= OWWfive Criteria n <br /> DkwkVFuran Mediod 23 <br /> train samples FkO surrogates Each fief sample 70%to 130%rewv ry NA Yes--Note 1 <br /> (spired in lab during armi blank <br /> pim"ration of}CAD for <br /> ssrriplit trains) <br /> Lab surrogates(inWnal Each fiW sample 40%to 130%recovery NA Yes--Nate 2 <br /> queu�titation standards) and blank ter tat whexaj <br /> 25%to 130%r wary <br /> (for hepta ) <br /> Laboratory reagent One XADifilter Levels less than lowest NA Yes--Note 3 ' <br /> blank calbttian standard <br /> Laboratory control One spiced 50%to 150% NA Yes <br /> sample(blank reagents XADltilter arc: <br /> spiked with <br /> independent standards <br /> of native DiaxinfFuran) <br /> Ind pendent(second After initial 80%to 12096 difference NA Yes--Note 4 F, <br /> soume)check standard calibrates <br /> (EPA or certified y <br /> Dioxln/Furan reference <br /> standards) <br /> Note 1--AS indicated in TaNe 5-10, sample SuffOqatO MOVedes were low for 13C 2A4,74-PeCDF. <br /> Note 2--As indicated in Tables-10,IOS toluene MW surrogate recoveries were low for various 13C compounds for Runs 6,By 9, <br /> and 10. ` <br /> Note 3--Criteria met for all 2,3,7,8 isomers in both method blanks with the 9xoqpWn of OCDD. <br /> Note criteria met for ag 2,3,7,8 isomers except for 1,2,3,7,$-PSCDF and 2,3,4,7,5-PeCDF in both spike checks and OCDF in <br /> the Bates 2 spike check. <br /> 4 <br /> K <br /> KM-AE"4951-0$-03 55.wo <br /> Y <br />