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Emission Test Report <br /> EMC WA-2-08 <br /> Section 5 <br /> Revision: 0 <br /> Date: September 30.1999 <br /> ?4 Page 5 of 18 <br /> Table 54 (Continued) <br /> Test Method of PrecWM <br /> parameters Matrix determinatlix n F Criteria mer <br /> llllOW 29 Analysis of bah sampW once to demon- NA NA Yes <br /> tram samples =nponer p strati systern <br /> frorrr fletd reagent oont d(no gross <br /> blanks contamination) <br /> and to determine <br /> blank cornection <br /> values <br /> C'C <br /> check sUmdard After to 110% 14 A yes <br /> Cued SWdard, calbmtIon GFAAS);90%to 110% <br /> 'ndependent of working a c c u ra cy(CVAAS) <br /> 4y <br /> callbrationstandards) <br /> Spiked lab reagent Two control spikes 5%to 135%recovery <40%RPD Yes <br /> FN.L blanks simula front- for each or analysed by standard <br /> arld back-halftrain omponent (or I&MIUM <br /> portents combined <br /> cwponorits)at <br /> least'lox the <br /> estimated <br /> detection I i m it <br /> ..4 2,articulate Meth 26A Balance calibration PrIOr to and after *.0.2 mg of Standard T v r o Yes <br /> flatter #teWront check with ASTM OUS all tare wirings weights aWWAU lIat g we g h i n g s, <br /> half rinses weights and graVkMtric `C931 t being weighed 6 hr apart <br /> determinations must agree <br /> within <br /> 0.5 mg <br /> Ij <br /> Mhl Method Duplicate analysis Each sample N A <5%RPp e s <br /> � 26A upl y � , <br /> impinger lotherwise <br /> w-=- contents repeat <br /> delicate <br /> analysis <br /> Spiked matrix samples 2 samples 90%to 110°► accuracy A Yes <br /> Yh (0.1 N H2SOJ (1 matrix) <br /> 4. ,e <br /> i <br /> MM-AED%R495i-%*3 S5.wpd <br />